圆柱形带壳推进剂装药枪击响应特性

为研究某圆柱形带壳推进剂装药的枪击响应特性,设计了一种12.7 mm子弹撞击试验。利用高速摄影机记录带壳装药在子弹撞击下的响应过程,并测试不同距离、方位处的空气超压及壳体破片速度,同时进行带壳装药在理想爆轰条件下的数值计算,得到了带壳装药的能量释放率。一共开展了四次圆柱形带壳装药的枪击试验,前三次装药发生了爆燃反应,第四次几乎无反应。结果表明:子弹撞击位置对圆柱形带壳装药的反应和能量释放率有较大影响,当子弹垂直入射带壳装药轴线后,推进剂发生点火、冒烟、熄火和低压燃烧的时序响应,其相对能量释放率为1.146%;而当子弹撞击位置偏离轴线一定距离时,推进剂几乎无反应,其相对能量释放率仅为0.473%;推进剂的反应对壳体破片有加速效应,带壳装药发生爆燃反应时的破片速度可达428.6 m·s~(-1),而几乎无反应时的最高破片速度仅有70.1 m·s~(-1)。     

Systematic study of Nd~(3+) on structural properties of ZnO nanocomposite for biomedical applications; in-vitro biocompatibility,bioactivity, photoluminescence and antioxidant properties

Owing to the inconformity in ionic radius between Nd~(3+) and Zn~(2+), the successful incorporation of Nd~(3+) ion into the ZnO nanocrystals still remains a great challenge. In the present study various doping ratios containing 1 wt%, 5 wt%, 7 wt% and 10 wt% of Nd~(3+) doped ZnO nanoparticles(Nd/ZnO NPs) were synthesized in which a bio-layer caped the NPs. SEM/EDX analysis was performed on the ZnO and Nd/ZnO NPs. In addition, the as-synthesized NPs were characterized using X-ray diffraction(XRD), dynamic light scattering(DLS), differential reflectance spectroscopy(DRS) and photoluminescence(PL) spectroscopy.The average size of Nd(5 wt%)/ZnO NPs was in the range of 6.22 and 15 e18 nm based on XRD and SEM techniques, respectively. The measured band gap values for pure ZnO and Nd/ZnO NCs with doping ratios of 1 wt%, 5 wt%, 7 wt% and 9 wt% were equal to 3.46, 3.26, 3.05, 3.25 and 3.29, respectively. After inhalation, nanoparticles first interact with lung surfactant system and accordingly their toxic effects will appear on lungs cells such as A549 cell line. The effect of Nd/ZnO NPs to interact by human A549 cell line was evaluated by means of cell viability test. According to cell viability test the concentrations of 0.3 and 0.5 mg/mL of Nd/ZnO NPs induce a low toxicity. The present study shows that these toxic effects of Nd/ZnO NPs can be rectified by capping its surface via the addition of a bio-layer around particles in order to prevent them from interacting A549 cell line.     

超级电容器的电性能及其在智能仪表上的应用

超级电容器作为一种新型储能元件,目前应用越来越广泛,但在很多细分市场还处于培育阶段,相关行业标准也不尽完善。文中以超级电容器的等效电路模型引出了电性能的特征参数,对比分析了主要标准中电性能特征参数测试方法的差异,提出了在智能仪表中应用超级电容器的要点,对全面认识超级电容器的电性能,在实际工作中正确的应用超级电容器,有一定的参考价值。     

Pressure transient analysis for asymmetrically fractured wells in dual-permeability organic compound reservoir of hydrogen and carbon

In this paper, a comprehensive semi-analytical model was presented to investigate pressure transient behavior for asymmetrically fractured wells in organic compound reservoir of hydrogen and carbon with dual-permeability behavior. Stehfest inversion algorithm can be used to transform it back into time domain to obtain pressure solution. The presented solution was validated well with numerical solutions. Flow characteristics for asymmetrically fractured wells in dual-permeability organic compound reservoir of hydrogen and carbon were divided into five regime. The effects of some important parameters on dimensionless pressure and its derivative curves were analyzed in details, including inter-porosity flow coefficient from matrix to natural fractures λ, storage coefficient ω, fracture asymmetry factor θ and permeability ratio κ. The presented model can be used to predict production performance and do well test analysis in the development of dual-permeability organic compound reservoir of hydrogen and carbon.     

载气热提取法测定熔敷金属中扩散氢收集条件的探究

探究了GB/T 3965—2012《熔敷金属中扩散氢测定方法》中载气热提取法收集条件对测定扩散氢含量的影响,并与水银法进行了对比。研究结果表明,样本炉温设定为400℃,A型试块的内部温度大约在51 min时稳定在358℃左右,B型试块内部温度大约在27 min时稳定在391℃左右;载气热提取法电信号曲线收集结束点的电信号及斜率均接近0时获得的结果与水银法具有较好的一致性。     

InSb红外探测器芯片粘接工艺研究

基于InSb红外探测器的封装特点,采用正交试验法研究了芯片粘接过程中基板平整度、粘接剂抽真空时间、配胶时间、固化条件等工艺参数对芯片性能及可靠性的影响。通过计算极差和方差分析了各因素对芯片可靠性的影响大小。结果表明,固化条件对粘接后芯片的性能影响最大,其次是配胶时间,而抽真空时间和基板平整度影响相对较小。针对极差分析得出的较优参数组合和较差参数组合,利用X射线衍射(XRD)研究了不同参数组合对晶片粘接的应力大小,所得结果与正交试验一致。     

Stiffness and strength characteristics of demolition waste,glass and plastics in railway capping layers

The increased generation of demolition waste has led to the successful implementation of its utilization in civil engineering projects. The combination of recycled aggregates and supplementary materials can potentially improve the quality of geomaterials when constructing alternative railway capping layers. In this research, two types of demolition waste, namely, Recycled Concrete Aggregates (RCA) and Crushed Brick (CB), were studied in comparison to two Conventional Capping Materials (CCMs), which are currently used for railway track construction. Recycled Glass (RG) and Mixed Recovered Plastic (MRP) were also blended with RCA to assess their performance. All the materials and mixtures were evaluated in terms of both stiffness and strength. A new Repeated Load Triaxial (RLT) testing protocol was introduced based on the stress induced in the capping layers to determine the stiffness of the materials. A comparison was made among the current resilient modulus prediction models to find a model that would better fit the results for the demolition waste and mixtures. Multistage triaxial tests were also conducted to determine the strength, friction, stiffness and energy absorption capacity of the materials. It was found from this research study that RCA, CB and mixtures of RCA with RG and MRP have equivalent or higher levels of stiffness and strength than CCMs and are suitable alternatives for sustainable railway capping layer construction.     

300M超高强钢在中性盐雾环境中的腐蚀行为及机制

摘要：为了研究300M超高强钢在中性盐雾环境中的腐蚀行为及腐蚀机制，采用失重法，宏观、微观腐蚀形貌分析，三维表面轮廓分析及电化学分析的研究方法，来表征腐蚀实验现象并进行分析。结果表明：300M超高强钢在中性盐雾环境中的腐蚀产物为FeOOH、Fe2O3、Fe(OH)3和Fe3O4；腐蚀速率随着腐蚀时间逐渐降低，腐蚀后期（72h）腐蚀速率降低50%；腐蚀初期以点蚀为主，点蚀坑通过横向扩展，逐渐发展为后期的均匀腐蚀，腐蚀表面形貌呈沟壑状；外腐蚀层对基体的保护能力很弱，Cr元素在锈层靠近基体的一侧偏聚使内腐蚀层具有一定的抗腐蚀性。     

Co/Al金属在聚晶立方氮化硼中的作用及加工适用性

通过正交试验和切削试验相结合的方法,检测聚晶立方氮化硼(PCBN)烧结体的硬度和强度,分析并观察烧结体组元相互熔渗状况以及微观形貌,探索了Co/Al金属对PCBN烧结体的影响以及不同结合剂含量PCBN的加工适应性。试验结果表明:CBN含量和Co含量对PCBN的抗弯强度和硬度影响显著;在刀具材料的选择上,高PCBN浓度的刀具适合加工灰铸铁,低PCBN浓度的刀具适合加工淬硬钢;Co/Al金属能够通过高温高压在PCBN层和硬质合金基体之间进行相互熔渗,导致PCBN层在距硬质合金10~20μm处Co含量达到最大值;PCBN的失效为穿晶断裂方式。     

不同层面倾角下锦屏一级水电站左岸板岩坡体破坏模式及能量特征

为了合理分析锦屏一级水电站左岸坡体的变形,选取坡体板岩进行巴西劈裂试验,分别研究了不同层面倾角下不同饱水率板岩的力学特性及能量特征。结果表明,板岩的抗拉强度随层面倾角的不断增加先减小后增加,其最大降幅达82%;同一层面倾角下,随着饱水程度的增加,板岩抗拉强度逐渐降低,在层面倾角为45°时,抗拉强度从1.64MPa降至0.52MPa,降幅达68%;试样层面倾角0°~90°的破坏受饱水率的影响较小,主要由层面倾角控制,破坏特征分为岩石拉伸型破坏、层面剪切破坏、基质-层面互剪型破坏、层面张拉破坏四种模式;试样破坏的累积能量随饱水程度的增加而不断减小,在相同饱水程度下,累积能量随层面倾角的增大而逐渐减小,累积能量的增长速率与荷载比成非线性关系,在轴向荷载达40%~80%时增长最快。